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Department of Process Engineering and Technology of Polymer and Carbon Materials

Sustainable Biomass and Bioproducts Engineering

Bio-Components Characterization (laboratory)

coordinator: prof. Joanna Wolska (e-mail)

The practicals will be carried out each week according to the SCHEDULE

Students should be prepared for a short test before each exercise. Both, the test as well as the rules of passing an exercise will be up to a teacher's decision, who will provide all the neceassary information before the classes.

Manuals:

Exercise 1: Chemical analysis, sampling and data analysis

Exercise 2: NMR analysis (remark: before attending the exercise students should put an extra attention to the calculation and re-calculation of concentrations as well as basics of NMR spectroscopy)

Exercise 3: UV-VIS spectroscopy, sample preparation, calibration

Exercise 4: IR and FTIR  analyses,  sample preparation, calibration (+ charts)

Exercise 5: Raman spectroscopy,  sample preparation, calibration (+ charts)

Exercise 6: Rheology and viscometry, sample preparation

Exercise 7: Surface analysis: contact angle and microscopy

Exercise 8: Molecular weight determination, viscometric method

Recovery of biocomponents (laboratory)

coordinator: dr Katarzyna Smolinska-Kempisty (e-mail)

SCHEDULE

Manuals:

Exercise 1: Extraction of residual elements from biomass

Exercise 2

Exercise 3

Exercise 4

Exercise 5

Exercise 6

Exercise 7: Solid-Liquid and Liquid-Liquid extraction of bioactive components

Exercise 8

Operation unit and reactors of biomass treatment I (laboratory)

coordinator: dr Anna Siekierka (e-mail)

SCHEDULE

Manuals:

Exercise 1: Purification of glycerol/water solutions from biodiesel synthesis

Exercise 2: Distillation and rectification of water-ethanol mixture

Exercise 3: Demineralization by electrodialysis and capacitive deionization

Exercise 4: Supercritical fluid extraction

Exercise 5: Separation of oil-water emulsion by nanofilters

Exercise 6: Carbonization of biomass

Exercise 7: Glucose fermentation

Exercise 8: Transesterification of vegetable oil

Exercise 9: Hydrolysis of starch (chemical vs. enzymatic process)

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